eagle-i Harvard UniversityHarvard University
See it in Search

Magnetic Resonance Laboratory (FAS)

Location: Naito Laboratory, Room B05, 12 Oxford Street, Cambridge, MA 02138

Summary:

Welcome to the Magnetic Resonance Facility of the Department of Chemistry and Chemical Biology, Harvard University, in the Laukien-Purcell Instrumentation Center.

Affiliations:

People:

Resources:

Instruments

  • Bruker Avance 700 NMR Spectrometer ( NMR instrument )

  • Bruker ESP 300E EPR spectrometer ( Electron paramagnetic resonance spectrometer )

    Operates at X-band frequency (9 GHz). Type of resonator: St9202.

  • Varian INOVA 500 (I500) NMR spectrometer ( NMR instrument )

    Frequency: 499.75 MHz.
    Number of probes: 2 (one 5 mm IDPFG and one 4mm nano-probe).
    Number of RF Channels: 2 (one H/F and one X).
    Magnet: Oxford actively-shielded magnet at 11.75 T Proton Resonance.

  • Varian INOVA 500 (I500B) NMR Spectrometer ( NMR instrument )

    Magnet: Oxford standard superconductive magnet at 11.75 T Proton Resonance Number of RF channels: 2 Number of probes: 3 (a 5 mm IDPFG, a 3 mm BB, and a CapNMR) Frequency: 500.21 MHz

  • Varian INOVA 500 (I500C) NMR spectrometer ( NMR instrument )

    Number of RF Channels: 2 (one H/F and one X).
    Number of probes: 2 (one 5 mm IDPFG and one 5 mm DBPFG probe).
    Magnet: Oxford actively-shielded magnet at 11.75 T.
    Proton Resonance Frequency: 499.75 MHz.

  • Varian INOVA 600 NMR Spectrometer ( NMR instrument )

    Proton Resonance Frequency: 599.78 MHz.
    Four RF channels available for triple resonance experiment with Deuterium decoupling.
    Field Strength: 14.1 T Standard superconducting magnet with low boil-off Dewar.
    Two probes available: 5 mm IDPFG (Indirect-Detection with z-Pulsed-Field-Gradient) and 4mm HRMAS nano-probe.

  • Varian Mercury 300 (M300) NMR spectrometer ( NMR instrument )

    Magnet: Oxford standard superconductive magnet at 7.1 T.
    Number of probes: 1 (5mm 4-nuc) tuned for observing H1, F19, and B11 NMR, but can be retuned to observe most of other rare nuclei upon request.

  • Varian Mercury 400 (M400) NMR spectrometer ( NMR instrument )

    Number of probes: 1 (5 mm 4-nuc) tuned to observe H1, F19, and C13.
    Magnet: Oxford standard magnet at 9.4 T.
    Proton Resonance Frequency: 400.02 MHz.

  • Varian Mercury 400 (M400B) NMR spectrometer ( NMR instrument )

    Proton Resonance Frequency: 399.86 MHz.
    Accessories: ASM auto sample changer.
    Magnet: Bruker Spectrospin standard magnet at 9.4 T.
    Number of probes: 1 (5 mm 4-Nuc) tuned to observe H1, F19, C13, and P31 NMR.
    Performa I pulse field gradient.

Protocols

  • gCOSY procotol ( Protocol )

    Protocol page includes detailed Instructions for gCOSY and several other kinds of 2D NMR experiments for the structural elucidation of organic molecules.

  • gHMBC protocol ( Protocol )

    Protocol page includes detailed Instructions for HMBC and several other kinds of 2D NMR experiments for the structural elucidation of organic molecules.

  • gHMQC protocol ( Protocol )

    Protocol page includes detailed Instructions for HMQC and several other kinds of 2D NMR experiments for the structural elucidation of organic molecules.

  • gHSQC protocol ( Protocol )

    Protocol page includes detailed Instructions for HSQC and several other kinds of 2D NMR experiments for the structural elucidation of organic molecules.

  • NOESY protocol ( Protocol )

    Type of 2D NMR Experiment.

  • ROESY protocol ( Protocol )

    Protocol for one of several useful 2D NMR experiments for structural elucidation of organic molecules.

  • TOCSY protocol ( Protocol )

    Protocol for one of several useful 2D NMR experiments for structural elucidation of organic molecules.

Services


Web Links:

Last updated: 2015-12-07T14:20:49.102-06:00

Copyright © 2016 by the President and Fellows of Harvard College
The eagle-i Consortium is supported by NIH Grant #5U24RR029825-02 / Copyright 2016